반응 #58457

ord-df7d5b74ebb24e72a670ebe62c3c5b72

반응 방정식

O=C(CBr)c1ccccc1
2-bromoacetophenone
O=C(O)CC1CCCCN1C(=O)OCc1ccccc1
2-carboxymethyl-piperidine-1-carboxylic acid benzyl ester
O=C(CC1CCCCN1C(=O)OCc1ccccc1)OCC(=O)c1ccccc1
title compound
O=C(CC1CCCCN1C(=O)OCc1ccccc1)OCC(=O)c1ccccc1
(RS)-2-(2-Oxo-2-phenyl-ethoxycarbonylmethyl)piperidine-1-carboxylic acid benzyl ester

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

The title compound (4.0 g) was prepared from 2-bromoacetophenone (2.20 g) and 2-carboxymethyl-piperidine-1-carboxylic acid benzyl ester according to the method of description 36

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07423052B2uspto-grants-2008_09