반응 #58261

ord-67d0165016824c9f88d8389d83c0600b

반응 방정식

COc1ccc(C(=O)c2ccc3c(c2)OCO3)c(C(=O)O)c1
2-(1,3-benzodioxol-5-yl)carbonyl-5-methoxybenzoic acid
NN.O
hydrazine hydrate
→
COc1ccc2c(-c3ccc4c(c3)OCO4)n[nH]c(=O)c2c1
4-(1,3-Benzodioxol-5-yl)-7-methoxy-2H-phthalazin-1-one

반응물

COc1ccc(C(=O)c2ccc3c(c2)OCO3)c(C(=O)O)c1
2-(1,3-benzodioxol-5-yl)carbonyl-5-methoxybenzoic acid
NN.O
hydrazine hydrate

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타This compound is obtained

실험 절차

This compound is obtained according to the procedure described in 1.2. by reacting 2-(1,3-benzodioxol-5-yl)carbonyl-5-methoxybenzoic acid unpurified with hydrazine hydrate.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07423030B2uspto-grants-2008_09