반응 #58113

반응 방정식

5-benzyloxy-8-(2,2-dihydroxy-acetyl)-4H-benzo[1,4]oxazin-3-one

1-(2,6-dimethyl-phenoxymethyl)-cyclopropylamine

trifluoroacetate

→

8-{2-[1-(2,6-dimethyl-phenoxymethyl)-cyclopropylamino]-1-hydroxy-ethyl}-5-hydroxy-4H-benzo[1,4]oxazin-3-one

반응 조건

후처리

1. 1
   기타Prepared

실험 절차

Prepared according to general method 3 from 329 mg (1 mmol) 5-benzyloxy-8-(2,2-dihydroxy-acetyl)-4H-benzo[1,4]oxazin-3-one and 191 mg (1 mmol) 1-(2,6-dimethyl-phenoxymethyl)-cyclopropylamine. Yield: 194 mg (49%, trifluoroacetate); mass spectroscopy: [M+H]+=399.

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