반응 #578427

ord-560fd31e74f546fc8b41f5b8ed44b5c6

용매

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타The target compound was obtained
  2. 2
    기타the procedure of Synthesis Example 1 aside
  3. 3
    기타in Synthesis Example 1
  4. 4
    추출for extraction

실험 절차

The target compound was obtained by following the procedure of Synthesis Example 1 aside from using bis(4-tert-butylphenyl) sulfoxide instead of the diphenyl sulfoxide and 4-tert-butylbromobenzene instead of the chlorobenzene in Synthesis Example 1, and increasing the amount of water for extraction.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07531290B2uspto-grants-2009_05