반응 #577226

ord-f3bc49ec10cc4ef4b3f6fa9e7b783d1e

반응 방정식

Cc1ccc(S(=O)c2ccc(C)cc2)cc1
bis(4-methylphenyl)sulfoxide
Cc1ccc(Cl)cc1
4-chlorotoluene
Cc1ccc([S+](c2ccc(C)cc2)c2ccc(C)cc2)cc1.[Cl-]
tris(4-methylphenyl)sulfonium chloride

용매

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타The target compound was obtained
  2. 2
    기타the procedure of Synthesis Example 1 aside
  3. 3
    기타in Synthesis Example 1
  4. 4
    추출for extraction

실험 절차

The target compound was obtained by following the procedure of Synthesis Example 1 aside from using bis(4-methylphenyl)sulfoxide instead of the diphenyl sulfoxide and 4-chlorotoluene instead of the chlorobenzene in Synthesis Example 1, and increasing the amount of water for extraction.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07527912B2uspto-grants-2009_05