반응 #573796

반응 방정식

compound

4-Fluoro-N-[2-(4-methoxybenzenesulfonamido)phenyl]benzamide

Lawesson reagent

→

title compound

수율 147.6%

4-Fluoro-N-[2-(4-methoxybenzenesulfonamido)phenyl]benzothioamide

수율 147.6%

용매

toluene

반응 조건

후처리

1. 1
   농축After the concentration
2. 2
   기타the residue was purified by silica gel column chromatography

실험 절차

A mixture of 549 mg (1.371 mmol) of the compound produced in Example 82, 333 mg (0.823 mmol) of Lawesson reagent and 10 ml of toluene was heated at 100° C. After the concentration, the residue was purified by silica gel column chromatography to obtain 506 mg of the title compound.

출처