반응 #571446

반응 방정식

dibenzylketone

dichlorobenzene

→

BISCYCLOPENTADIENE

용매

hexane

반응 조건

후처리

1. 1
   여과the solid product is filtered
2. 2
   세척washed with hexane
3. 3
   기타dried
4. 4
   기타Purification of this product
5. 5
   기타may be carried out by recrystallization from acetone or methyl ethyl ketone

실험 절차

A one mole equivalent sample of product II and two mole equivalent of dibenzylketone is heated for 4 hours in a mechanically stirred dichlorobenzene solution. The mixture is diluted with addition of hexane and the solid product is filtered, washed with hexane and dried. Purification of this product may be carried out by recrystallization from acetone or methyl ethyl ketone. ##STR41## where: Ph=phenyl rings.

출처