반응 #56976

ord-60b865b84fbc49f9851229edfdc10c8e

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

N-(6-Bromo-2,3,4,9-tetrahydro-1H-carbazol-1-yl)-2-methylbenzamide was prepared from 6-bromo-2,3,4,9-tetrahydro-1H-carbazol-1-amine and o-toluoyl chloride in a similar manner as described above to give a gray solid (19% yield). 1H-NMR (DMSO-d6): δ 11.01 (s, 1H), 8.70 (d, 1H), 7.59 (m, 1H), 7.47 (d, 1H), 7.33 (m, 2H), 7.26 (m, 2H), 7.17 (dd, 1H), 5.34 (m, 1H), 2.65 (m, 2H), 2.42 (s, 3H), 2.07 (m, 2H), 1.87 (m, 2H); MS m/z 383 (M−1).

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07419997B2uspto-grants-2008_09