반응 #56829

반응 방정식

5-chloro-2-methoxy-benzimidic acid ethyl ester

ammonia

→

5-chloro-2-methoxy-benzylideneamine

수율 129.0%

용매

methanol

반응 조건

후처리

1. 1
   기타Evaporation of volatiles under reduced pressure

실험 절차

A mixture of 5-chloro-2-methoxy-benzimidic acid ethyl ester (1.0 g, 4.0 mmol) and a solution of ammonia in methanol (7.0 M, 50 ml) was stirred for 48 hours. Evaporation of volatiles under reduced pressure provided 5-chloro-2-methoxy-benzylideneamine (0.875 g, 99% yield).

출처