반응 #565480
ord-a2bc46c6315442c19bb82f7cc6e4f1ea
반응 방정식
product
2H-pyran-3,5(4H,6H)-dione
product
3-iodo-4-methylbenzaldehyde
methyl 3-aminocrotonate
→
title compound
수율 45.5%
Methyl 4-(3-iodo-4-methylphenyl)-2-methyl-5-oxo-4,5,6,8-tetrahydro-1H-pyrano[3,4-b]pyridine-3-carboxylate
수율 45.5%
용매
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
The product from Example 11B (0.34 g, 3.0 mmol), the product from Example 54A (0.74 g, 3.0 mmol) and methyl 3-aminocrotonate (0.35 g, 3.0 mmol) in methanol (8 mL) were processed as described in Example 68A to provide the title compound (0.60 g).