반응 #565233

반응 방정식

2-chloromethyl quinoline

amino guanidine bicarbonate

→

product

수율 65.0%

2-[1-[3-(2-Quinolinylmethoxy)phenyl]ethylidene]hydrazinecarboximidamide

수율 65.0%

반응 조건

후처리

1. 1
   기타is prepared (13.1 g, m.p. 57°-59° C., 47% yield)

실험 절차

In a similar manner to Example 1A and using 2-chloromethyl quinoline, 3-(2-quinolinylmethoxy)acetophenone is prepared (13.1 g, m.p. 57°-59° C., 47% yield). This product is reacted with amino guanidine bicarbonate as in 1B above to give 2.35 g of product (65% yield), m.p. 168°-170° C.

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