반응 #564544
ord-cee0fac92b024bf0a2fbecaef95e916c
반응 방정식
반응물
시약
없음
용매
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
The procedure is as in Example 29 for the preparation of ethyl (4-methylbenzylthio)acetate, starting with iodoethane (10.5 g), a 2M ethanolic solution of sodium ethylate (37 cc) and ethyl 2-mercaptoacetate (8.1 g) in ethanol (100 cc). Ethyl (ethylthio)acetate (6.9 g) is thereby obtained, and is used in the crude state in the subsequent syntheses.