반응 #56163

반응 방정식

1,8-Diaminonaphthalene

p-Trifluoromethoxybenzoyl fluoride

→

2-(p-TRIFLUOROMETHOXYPHENYL)-1H-PERIMIDINE HYDROFLUORIDE

용매

toluene

toluene

반응 조건

후처리

1. 1
   기타of toluene, then decanted
2. 2
   workup.ADDITIONBoth solutions were added simultaneously to 25 ml

실험 절차

1,8-Diaminonaphthalene (1.52 grams; 0.0096 mole) was dissolved in 25 ml. of toluene, then decanted. p-Trifluoromethoxybenzoyl fluoride (2.0 grams; 0.0096 mole) was dissolved in 25 ml. of toluene. Both solutions were added simultaneously to 25 ml. of toluene. After the reaction mixture had been stirred for approximately 4 hours, TLC indicated that the reaction was complete.

출처