반응 #56162

반응 방정식

1,8-Diaminonaphthalene

m-trifluoromethylbenzoyl chloride

→

2-(m-trifluoromethylphenyl)-1H-perimidine hydrochloride

수율 95.4%

반응 조건

후처리

1. 1
   기타yielding 33.3 g

실험 절차

1,8-Diaminonaphthalene (15.82 g.; 0.10 mole) and m-trifluoromethylbenzoyl chloride (20.8 g.; 0.10 mole) were reacted in the same procedures as reported in Example 1, yielding 33.3 g. (95.4% yield) of 2-(m-trifluoromethylphenyl)-1H-perimidine hydrochloride, m.p. 280° C. (dec), mass spectrum m/e 312.

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