반응 #56136

ord-3418da2fcc3940ee9a213879cf40f87d

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

4-methoxy-2,6-dimethyl-3-ethyl-benzyl-triphenyl-phosphonium chloride is condensed with 7-formyl-3-methyl-octa-2,4,6-trien-1-oic acid ethyl ester to produce 9-(4-methoxy-2,6-dimethyl-3-ethyl-phenyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-oic acid ethyl ester which is converted by the procedure of Example 7 to form 9-(4-methoxy-2,6-dimethyl-3-ethyl-phenyl)-3,7-dimethyl-nona-2,4,6,8-tetraen-1-oic acid, m.p.: 197°-198° C.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04224244uspto-grants-1980_09