반응 #5588
ord-1a30f638e6c14bbab25c98517e050aa1
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1여과filtered
- 2농축concentrated
실험 절차
A solution of dicyclohexylamine (19.92 ml, 0.10 mole) and triethylamine (27.88 ml, 0.20 mole) in ethyl ether (100 ml) was cooled to 0° C. A solution of acryloyl chloride (7.93 ml, 0.1 mole) in ethyl ether (20 ml) was added and the solution was stirred for 12 hours, filtered and concentrated to obtain the product as a solid which was dried in vacuo. The structure was confirmed by NMR.