반응 #55830

ord-aedc70c75b4d444fa440641f5a47f82b

반응 방정식

NCCCSc1ncco1
2-(3-aminopropylthio)oxazole
CSC(=N)N[N+](=O)[O-]
S-methyl-N-nitroisothiourea
N=C(NCCCSc1ncco1)N[N+](=O)[O-]
N-nitro-N'-[3-(2-oxazolyl)thiopropyl]guanidine

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

Reacting 2-(3-aminopropylthio)oxazole with S-methyl-N-nitroisothiourea by the procedure of Example 2(ii) gives N-nitro-N'-[3-(2-oxazolyl)thiopropyl]guanidine. Similarly, reaction of the same starting material with N,S-dimethyl-N'-nitroisothiourea by the procedure of Example 2(iii) gives N-methyl-N'-nitro-N"-[3-(2-oxazolyl)thiopropyl]guanidine.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04221802uspto-grants-1980_09