반응 #55822

반응 방정식

N,S-dimethyl-N'-nitroisothiourea

3-[(2-aminoethyl)thiomethyl]isothiazole

S-methyl-N-nitroisothiourea

N-[2-(3-isothiazolylmethylthio)ethyl]-N'-nitroguanidine

→

N-[2-(3-isothiazolylmethylthio)ethyl]-N'-methyl-N"-nitroguanidine

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후처리

1. 1
   기타gives

실험 절차

Reacting 3-[(2-aminoethyl)thiomethyl]isothiazole with S-methyl-N-nitroisothiourea by the procedure of Example 2(ii) gives N-[2-(3-isothiazolylmethylthio)ethyl]-N'-nitroguanidine and reaction of the same starting material with N,S-dimethyl-N'-nitroisothiourea by the procedure of Example 2(iii) gives N-[2-(3-isothiazolylmethylthio)ethyl]-N'-methyl-N"-nitroguanidine.

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