반응 #55793

ord-11d198f4b413447f81bbe156e0edcc63

반응 방정식

NCCSCc1cccnn1
3-[(2-aminoethyl)thiomethyl]-pyridazine
CSC(=N)N[N+](=O)[O-]
S-methyl-N-nitroisothiourea
N=C(NCCSCc1cccnn1)N[N+](=O)[O-]
N-nitro-N'-[2-(3-pyridazinylmethylthio)ethyl]guanidine

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

Reaction of 3-[(2-aminoethyl)thiomethyl]-pyridazine with S-methyl-N-nitroisothiourea by the procedure of Example 2(ii) gives N-nitro-N'-[2-(3-pyridazinylmethylthio)ethyl]guanidine. Similarly, by the procedure of Example 2(iii), there is obtained N-methyl-N'-nitro-N"-[2-(3-pyridazinylmethylthio)ethyl]-guanidine.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04221802uspto-grants-1980_09