반응 #55787

ord-29edbbdb9ae548f9aa805056bad10ae3

반응 방정식

NCCSCc1cnccn1
2-[(2-aminoethyl)thiomethyl]pyrazine
CSC(=N)N[N+](=O)[O-]
S-methyl-N-nitroisothiourea
N=C(NCCSCc1cnccn1)N[N+](=O)[O-]
N-nitro-N'-[2-(2-pyrazinylmethylthio)ethyl]guanidine

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

Reaction of 2-[(2-aminoethyl)thiomethyl]pyrazine with S-methyl-N-nitroisothiourea by the procedure of Example 2(ii) gives N-nitro-N'-[2-(2-pyrazinylmethylthio)ethyl]guanidine. Similarly by the procedure of Example 2 (iii), there is prepared N-methyl-N'-nitro-N"-[2-(2-pyrazinylmethylthio)ethyl]guanidine.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04221802uspto-grants-1980_09