반응 #55665

ord-c69af58343e5484282070668dfb95f59

반응 방정식

CSC(NCCSCc1[nH]cnc1C)=C(C#N)S(=O)(=O)c1ccccc1
product
CSC(NCCSCc1[nH]cnc1C)=C(C#N)S(=O)(=O)c1ccccc1
1-Benzenesulfonyl-1-cyano-2-methylthio-2-{2-[(4-methyl-1H-imidazol-5-yl)methylthio]ethylamino}ethylene
C#CCN
propargylamine
→
C#CCNC(NCCSCc1[nH]cnc1C)=C(C#N)S(=O)(=O)c1ccccc1
title product
C#CCNC(NCCSCc1[nH]cnc1C)=C(C#N)S(=O)(=O)c1ccccc1
1-Benzenesulfonyl-1-cyano-2-(2-propynylamino)-2-{2-[(4-methyl-1H-imidazol-5-yl)methylthio]ethylamino}ethylene

반응물

CSC(NCCSCc1[nH]cnc1C)=C(C#N)S(=O)(=O)c1ccccc1
product
CSC(NCCSCc1[nH]cnc1C)=C(C#N)S(=O)(=O)c1ccccc1
1-Benzenesulfonyl-1-cyano-2-methylthio-2-{2-[(4-methyl-1H-imidazol-5-yl)methylthio]ethylamino}ethylene
C#CCN
propargylamine

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

The product of Step A is reacted with a four-fold excess of propargylamine according to the general procedure of Example 2, and the title product is produced.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04221737uspto-grants-1980_09