반응 #55656

ord-84ea0d37cd7e4ceea09e7d996fe0f21e

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타The crude product is recrystallized from n-hexane

실험 절차

13 g. of 3-nitro-4-chloro-benzophenone are reacted with 15 ml. of N-ethyl-N-cyclohexylamine as described in Example 2. The crude product is recrystallized from n-hexane to yield 15.3 g of pure, crystalline 3-nitro-4-(N-ethyl-N-cyclohexylamino)-benzophenone; m.p. 91.5°-92° C.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04221739uspto-grants-1980_09