반응 #554582

반응 방정식

hydrogen

2,4-Dimethyl-5-phenyl-pentanol

→

5-cyclohexyl-2,4-dimethyl-pentanol

수율 99.5%

용매

cyclohexane

반응 조건

후처리

1. 1
   기타The catalyst was removed
2. 2
   workup.DISTILLATIONthe product distilled

실험 절차

100 g of 2,4-Dimethyl-5-phenyl-pentanol (obtained as described in EP 0 908 439) combined with 2 g Ru on aluminium oxide (Ru content: 5 wt. %) were hydrogenated in 80 ml cyclohexane at a hydrogen pressure of 22 bar and at a temperature of 105° C. After 18 hours the reaction was finished. The catalyst was removed and the product distilled. 100 g (content: 99.5%) of 5-cyclohexyl-2,4-dimethyl-pentanol were obtained.

출처