반응 #554581
ord-956fe17f6170423684ccc3549d6672c7
반응 방정식
5-(4-Isopropylphenyl)-2-methyl-1-pentanol
hydrogen
→
5-(4-isopropylcyclohexyl)-2-methyl-1-pentanol
수율 99.7%
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타The catalyst was removed
- 2workup.DISTILLATIONthe product distilled
실험 절차
100 g of 5-(4-Isopropylphenyl)-2-methyl-1-pentanol (obtained as described in EP 0 908 439) combined with 1.5 g Ru on aluminium oxide (Ru content 5 wt. %) were hydrogenated at a hydrogen pressure of 25 bar and at a temperature of 110° C. After 15 hours the reaction was finished. The catalyst was removed and the product distilled. 100 g (content 99.7%) of 5-(4-isopropylcyclohexyl)-2-methyl-1-pentanol were obtained.