반응 #554581

ord-956fe17f6170423684ccc3549d6672c7

반응 방정식

CC(CO)CCCc1ccc(C(C)C)cc1
5-(4-Isopropylphenyl)-2-methyl-1-pentanol
[H][H]
hydrogen
CC(CO)CCCC1CCC(C(C)C)CC1
5-(4-isopropylcyclohexyl)-2-methyl-1-pentanol
수율 99.7%

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타The catalyst was removed
  2. 2
    workup.DISTILLATIONthe product distilled

실험 절차

100 g of 5-(4-Isopropylphenyl)-2-methyl-1-pentanol (obtained as described in EP 0 908 439) combined with 1.5 g Ru on aluminium oxide (Ru content 5 wt. %) were hydrogenated at a hydrogen pressure of 25 bar and at a temperature of 110° C. After 15 hours the reaction was finished. The catalyst was removed and the product distilled. 100 g (content 99.7%) of 5-(4-isopropylcyclohexyl)-2-methyl-1-pentanol were obtained.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08623340B2uspto-grants-2014_01