반응 #55386

반응 방정식

3-mercapto-1,2,4-triazole

3-aminopropanol

hydrobromic acid

→

3-(3-aminopropylthio)-1,2,4-triazole dihydrobromide

반응 조건

후처리

1. 1
   온도under reflux for 24 hours
2. 2
   기타The reaction mixture is evaporated to dryness
3. 3
   기타the residue recrystallised from ethanol/ether

실험 절차

A solution of 3-mercapto-1,2,4-triazole and 3-aminopropanol in hydrobromic acid is heated under reflux for 24 hours. The reaction mixture is evaporated to dryness and the residue recrystallised from ethanol/ether to give 3-(3-aminopropylthio)-1,2,4-triazole dihydrobromide.

출처