반응 #55334

ord-7dbf822835bd4ba1b6edb635d46894d6

반응 방정식

FB(F)F
BF3
ClCC1CO1
glycerol epichlorhydrin
CCCCCCCCCCCCO
dodecanol
CCCCCCCCCCCCOCCCCCCCCCCCC
Dodecyl ether
O/C=C\CCl
polyepichlorohydrin

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

185 g of glycerol epichlorhydrin are reacted with one mole, i.e., 186 g of dodecanol at 75°-80° C. in the presence of 1.5 ml of an acetic acid complex containing 36% BF3. Dodecyl ether of polyepichlorohydrin having the following formula is obtained:

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04220602uspto-grants-1980_09