반응 #55225
ord-4129a79c50954f558d8ed51230099002
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타hydrogenated at 20°
- 2여과Filtering
- 3기타evaporating
실험 절차
2.78 g. of 3-(2',4'-difluoro-4-biphenylyl)butane-1,3-diol are dissolved in 30 ml. of acetic acid and hydrogenated at 20° and under 1 atmosphere on 0.5 g. of 10% Pd-C until the reaction has ceased. Filtering and evaporating gives 3-(2',4'-difluoro-4-biphenylyl)butan-1-ol.