반응 #55192

ord-edcb1023a5214e3eb85b16d8b4b1cb68

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    온도under reflux for 2 hours
  2. 2
    workup.ADDITIONthe mixture is poured onto ice

실험 절차

1 g. of 3-(2',4'-dibromobiphenylyl)-3-hydroxybutyric acid and 10 ml. of acetic anhydride are heated under reflux for 2 hours and the mixture is poured onto ice and worked up in the customary manner to give 3-(2',4'-dibromo-4-biphenylyl-2-butenoic acid.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04151302uspto-grants-1979_04