반응 #55185

반응 방정식

thionyl chloride

3-(2',4'-difluoro-4-biphenylyl)butyric acid

→

3-(2',4'-difluoro-4-biphenylyl)butyryl chloride

용매

benzene

반응 조건

후처리

1. 1
   기타the mixture is evaporated under reduced pressure

실험 절차

6 g. of thionyl chloride and 10 g. of 3-(2',4'-difluoro-4-biphenylyl)butyric acid in 80 ml. of benzene are allowed to stand at 25° for 24 hours and the mixture is evaporated under reduced pressure to give 3-(2',4'-difluoro-4-biphenylyl)butyryl chloride.

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