반응 #55181

반응 방정식

3-(2',4'-difluoro-4-biphenylyl)butyric acid

H2SO4

→

3-(2',4'-difluoro-4-biphenylyl)butyric acid n-butyl ester

용매

n-butanol

반응 조건

후처리

1. 1
   온도under reflux with 1 ml
2. 2
   기타The mixture is evaporated
3. 3
   세척the chloroform solution is washed with NaHCO3 solution
4. 4
   기타dried
5. 5
   기타evaporated

실험 절차

2 g. of 3-(2',4'-difluoro-4-biphenylyl)butyric acid are heated under reflux with 1 ml. of concentrated H2SO4 and 30 ml. of n-butanol for 7 hours. The mixture is evaporated and taken up in chloroform and the chloroform solution is washed with NaHCO3 solution, dried and evaporated to give 3-(2',4'-difluoro-4-biphenylyl)butyric acid n-butyl ester.

출처