반응 #55120

ord-4a997f7fe7a64c599a73e9e0d01ada42

반응 방정식

NCCSCc1ncccn1
2-[(2-aminoethyl)thiomethyl]pyrimidine
O=C(N=C=S)c1ccccc1
benzoyl isothiocyanate
O=C(NC(=S)NCCSCc1ncccn1)c1ccccc1
N-benzoyl-N'-[2-(2-pyrimidylmethylthio)ethyl]thiourea

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

By the procedure of Example 18, 2-[(2-aminoethyl)thiomethyl]pyrimidine is reacted with benzoyl isothiocyanate to give N-benzoyl-N'-[2-(2-pyrimidylmethylthio)ethyl]thiourea. Removing the benzoyl group by the procedure of Example 18 gives N-[2-(2-pyrimidylmethylthio)ethyl]thiourea.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04151288uspto-grants-1979_04