반응 #550223
ord-3087bf949a194fdb9c900eb94a64657a
반응 방정식
crotonyl chloride
carnitine hydrochloride
ethyl ether
→
crotonoyl carnitine
반응 조건
온도
50°CELSIUS
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타a precipitate formed
- 2여과The precipitate was filtered off
- 3기타such in the subsequent reaction
실험 절차
8 cc (0.08 moles) of crotonyl chloride were added to a solution of carnitine hydrochloride (8 grams; 0.04 moles) in trifluoroacetic acid. The reaction mixture was kept under stirring at 50° C. overnight. Subsequently, ethyl ether was added to the mixture and a precipitate formed. The precipitate was filtered off and used as such in the subsequent reaction.