반응 #55013

반응 방정식

ethyl 4-oxo-1-piperidinecarboxylate

2-pyrimidinamine

methylbenzene

→

ethyl 4-(2-pyrimidinylimino)-1-piperidinecarboxylate

용매

water

반응 조건

후처리

1. 1
   기타The reaction mixture is evaporated

실험 절차

A mixture of 34 parts of ethyl 4-oxo-1-piperidinecarboxylate, 20 parts of 2-pyrimidinamine, 8 drops of acetic acid and 90 parts of methylbenzene is stirred and refluxed for 28 hours with water-separator. The reaction mixture is evaporated, yielding 50 parts of ethyl 4-(2-pyrimidinylimino)-1-piperidinecarboxylate as a residue.

출처