반응 #54875

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product

Ethyl 4-(4-Acetyl-4-ethoxycarbonyl-8-acetoxy-8-methyltridecyl)benzoate

ethyl 4-(4-acetyl-4-ethoxycarbonyl-8-acetoxytridec-6-en-1-yl)benzoate

→

4-(4-Acetyl-8-hydroxy-8-methyltridecyl)benzoic Acid

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후처리

1. 1
   기타This compound is prepared by the method
2. 2
   기타The title compound is purified by column chromatography on silica gel with 4% methanol in chloroform as eluant
3. 3
   기타is obtained as a nearly colorless, viscous oil

실험 절차

This compound is prepared by the method described in Example 3, Step C, except that an equivalent quantity of the product of Step B of the present example replaces ethyl 4-(4-acetyl-4-ethoxycarbonyl-8-acetoxytridec-6-en-1-yl)benzoate. The title compound is purified by column chromatography on silica gel with 4% methanol in chloroform as eluant and is obtained as a nearly colorless, viscous oil.

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