반응 #548203
ord-5b278b0be4584379833361726e6a865c
반응 방정식
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1온도The mixture is then cooled
- 2기타the resulting solid is collected
- 3세척washed with ether
- 4기타recrystallized from methanol-acetone
실험 절차
A slurry of 15.9 g (0.08 mole) of p-chlorophenethylamine hydrochloride in 25 ml of O-methylcaprolactim is allowed to stand at room temperature 3 days with occasional stirring with a glass rod. The mixture is then cooled and the resulting solid is collected, washed with ether and recrystallized from methanol-acetone to give 2-(p-chlorophenylethylimino)hexahydroazapine hydrochloride.