반응 #54666

반응 방정식

p-menth-3-oyl chloride

glycine propyl ester hydrochloride

sodium bicarbonate

→

N-p-Menth-3-oylglycine n-propyl ester

반응 조건

후처리

1. 1
   workup.DISTILLATIONThe crude product was distilled b.p. 170°/0.1 mm
2. 2
   workup.DISTILLATION(After distillation the product

실험 절차

Following the procedure of Example 2 p-menth-3-oyl chloride (2.0 g., 0.01 moles), was reacted with glycine propyl ester hydrochloride (1.5 g., 0.01 moles) and sodium bicarbonate (1.6 g., 0.02 moles). The crude product was distilled b.p. 170°/0.1 mm. (After distillation the product rapidly solidifies). (Found, C: 68.2; H: 1016; N: 5.0. C16H29NO3 requires, C: 67.8; H: 10.6; N: 4.9.)

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