반응 #54539

ord-8367b4439f8d48dd9ed4645acc334bc3

반응 방정식

CC(=O)OC1CCN([C@H]2CCCC[C@H]2N)C1
cis-N-[2-(3-acetyloxy-1-pyrrolidinyl)cyclohexyl]amine
Cc1cc(C)cc(C(=O)Cl)c1
3,5-dimethylbenzoyl chloride
→
CC(=O)OC1CCN([C@H]2CCCC[C@H]2NC(=O)c2cc(C)cc(C)c2)C1
cis-N-[2-(3-acetyloxy-1-pyrrolidinyl)cyclohexyl]-3,5-dimethylbenzamide

반응물

CC(=O)OC1CCN([C@H]2CCCC[C@H]2N)C1
cis-N-[2-(3-acetyloxy-1-pyrrolidinyl)cyclohexyl]amine
Cc1cc(C)cc(C(=O)Cl)c1
3,5-dimethylbenzoyl chloride

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

Following the procedure of Example 1b, using cis-N-[2-(3-acetyloxy-1-pyrrolidinyl)cyclohexyl]amine and 3,5-dimethylbenzoyl chloride there is obtained as product cis-N-[2-(3-acetyloxy-1-pyrrolidinyl)cyclohexyl]-3,5-dimethylbenzamide.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04148914uspto-grants-1979_04