반응 #54457

ord-6333a963d3394b99b77cf09e5bae714e

반응 방정식

Cl.Cl.Cl.[O]=[V]
vanadium oxytrichloride
O[Si](c1ccc(Br)cc1)(c1ccc(Br)cc1)c1ccc(Br)cc1
tri (p-bromophenyl) silanol
→
Brc1ccc([SiH2][O][V+2]([O][SiH2]c2ccc(Br)cc2)[O][SiH2]c2ccc(Br)cc2)cc1.[O-2]
tris[(p-bromophenyl)-siloxy]-vanadium oxide

반응물

Cl.Cl.Cl.[O]=[V]
vanadium oxytrichloride
O[Si](c1ccc(Br)cc1)(c1ccc(Br)cc1)c1ccc(Br)cc1
tri (p-bromophenyl) silanol

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

vanadium oxytrichloride was reacted with tri (p-bromophenyl) silanol, (m.p.= 120°-121° C.) to produce tris[(p-bromophenyl)-siloxy]-vanadium oxide (m.p.= 175° C.); and

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04148829uspto-grants-1979_04