반응 #54447

ord-4b0992e459a24daaa1b21148f6ab2d51

반응 방정식

CCCCCCCCCCCCCCCCCC(=O)Cl
stearoyl chloride
ClCl
chlorine
O=S(=O)(O)Cl
ClSO3H
N#CC(C#N)=c1ccc(=C(C#N)C#N)cc1
TCNQ
→
CCCCCCCCCCCCCCCCC(Cl)C(=O)Cl
2-chlorostearoyl chloride

반응물

CCCCCCCCCCCCCCCCCC(=O)Cl
stearoyl chloride
ClCl
chlorine
O=S(=O)(O)Cl
ClSO3H
N#CC(C#N)=c1ccc(=C(C#N)C#N)cc1
TCNQ

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    workup.DISTILLATIONThe product is distilled

실험 절차

Following the procedure of Example I, stearoyl chloride is reacted with chlorine in the presence of ClSO3H and TCNQ. The product is distilled to provide substantially pure 2-chlorostearoyl chloride.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04148811uspto-grants-1979_04