반응 #54426

ord-a53ff6c8c28446308ef622c6f91f85ff

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

As in Example 17, reaction of o-chloro-β-nitrostyrene with dimethylammonium dimethyldithiocarbamate in the presence of carbon disulfide gave o-chloro-α-(nitromethyl)benzyl dimethyldithiocarbamate melting at 102° C.-103.5° C. when recrystallized without heating from acetone-methanol solution.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04148795uspto-grants-1979_04