반응 #54209

ord-160d52d13306401890cc3c52431d6e5b

반응 방정식

O=[N+]([O-])c1ccccc1
Nitrobenzene
CC(C)=O
acetone
→
CC(=O)c1ccc(-c2cccc(-c3ccccc3)c2)cc1
crude product
CC(=O)c1ccc(-c2cccc(-c3ccccc3)c2)cc1
4-acetyl m-terphenyl

반응물

O=[N+]([O-])c1ccccc1
Nitrobenzene
CC(C)=O
acetone

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    여과After filtration
  2. 2
    기타the acetone evaporation

실험 절차

Nitrobenzene is stripped with steam and the solid residue is dissolved into acetone. After filtration and the acetone evaporation, 400 g of crude product is obtained.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04147728uspto-grants-1979_04