반응 #5396
ord-445013eb9d6b4372b91d441d2c130c81
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1workup.ADDITIONis introduced the monomer system
- 2기타prepared separately
- 3workup.STIRRINGby stirring (350 rpm) for 10 hours at 80° C.
실험 절차
It is stirred at room temperature for 30 minutes and then is introduced the monomer system prepared separately consisting of g 100 of styrene, g 67.5 of divinylbenzene (50%) in toluene (225 ml) and n-octane (75 ml) containing 3 g of benzoyl peroxide. The polymerization is carried out by stirring (350 rpm) for 10 hours at 80° C.