반응 #53793

반응 방정식

product

5-(1H-Indol-2-yl)-2-methoxy-phenylamine

5-(1H-indol-2-yl)-2-methoxy-phenylamine

thiophosgene

→

[5-(1H-indol-2-yl)-2-methoxy-phenyl]-isothiocyanate

반응 조건

실험 절차

The product from Example 1, 5-(1H-indol-2-yl)-2-methoxy-phenylamine, (4.76 g, 20 mmol) was reacted with thiophosgene (1.9 mL, 25 mmol) according to the procedure for Example 23, Step A, to give [5-(1H-indol-2-yl)-2-methoxy-phenyl]-isothiocyanate (4.55 g), as a black solid.

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