반응 #53760

ord-868776c4aa2e4da9aec0e9e64cce3e8d

반응 방정식

[F-].[Na+]
sodium fluoride
[F-].[Na+]
sodium fluoride
CC#N
acetonitrile
COCCOC
dimethoxyethane
OCc1ccccc1
benzyl alcohol
O=C(F)OCc1ccccc1
Benzyl Fluoroformate

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

The process is performed as in Example 1 with, in the first reactor, 168 g (4 mol) of sodium fluoride powder having the same characteristics as described in Example 1 and 320 ml of acetonitrile and, in the second reactor, 108 g (1 mol) of benzyl alcohol, 50.5 g (1.2 mol) of sodium fluoride of the same characteristics as above and 150 g of dimethoxyethane.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US06858751B1uspto-grants-2005_02