반응 #5372

반응 방정식

Phenol

hexadecene

→

mono-hexadecylphenol

반응 조건

후처리

1. 1
   여과The ion exchange resin was filtered off
2. 2
   workup.DISTILLATIONthe excessive phenol and hexadecene were distilled off under reduced pressure
3. 3
   workup.DISTILLATIONAfter distillation under reduced pressure

실험 절차

Phenol (376 g, 4 mol), hexadecene (α-olefin) (449 g, 2 mol) and ion exchange resin (trade-mark: Dia-ion RCP-145HD) (34 g) were charged in a reactor and stirred at 110° C. for 2 hours. The ion exchange resin was filtered off and the excessive phenol and hexadecene were distilled off under reduced pressure. After distillation under reduced pressure, mono-hexadecylphenol was obtained. The yield was 510 g.

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