반응 #53313

반응 방정식

Triethylamine

Ethyl 4-(3-(2,6-dimethylbenzyloxy)phenyl)-4-bromobutyrate

→

title compound

Ethyl 4-(3-(2,6-dimethylbenzyloxy)phenyl)-3-butenoate

용매

carbon tetrachloride

반응 조건

후처리

1. 1
   여과the mixture can be filtered through a pad of silica gel few times
2. 2
   농축concentrate

실험 절차

Add Triethylamine to a solution of Ethyl 4-(3-(2,6-dimethylbenzyloxy)phenyl)-4-bromobutyrate (Step E) in carbon tetrachloride. After stirring approximately for 4 hours, the mixture can be filtered through a pad of silica gel few times, and concentrate to give the title compound.

출처