반응 #531805
ord-cda1e91de3df47838ccda7975c2a3996
반응 방정식
tris(3-(tert-butoxycarbonylamino)propyl)nitromethane
Tris(3-(tertbutoxycarbonylamino)propyl)nitromethane
trifluoroacetic acid
→
title compound 10c
수율 100.0%
Tris(3-aminopropyl)nitromethane trifluoroacetate salt
수율 100.0%
반응물
시약
없음
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1농축The reaction was then concentrated under high vacuum
실험 절차
A mixture of tris(3-(tert-butoxycarbonylamino)propyl)nitromethane 1c (10 g, 18.8 mmol) in trifluoroacetic acid (20 ml) and dichloromethane (50 ml) was stirred at room temperature for 4 h. The reaction was then concentrated under high vacuum to afford the title compound 10c (10.8 g, 18.8 mmol. 100%) as a gum.