반응 #531791

반응 방정식

Mercaptopropionic acid

Triphenylmethylchloride

→

3-(tritylthio)propionic acid

수율 95.7%

용매

methylene chloride

반응 조건

후처리

1. 1
   기타were carried out at room temperature
2. 2
   여과was gathered by filtration
3. 3
   기타the solid components obtained here
4. 4
   기타were dried under reduced pressure

실험 절차

Mercaptopropionic acid 12 (3.14 g) was dissolved in 50 ml of methylene chloride. Triphenylmethylchloride 13 (8.36 g) was added to that, and 19-hour reactions were carried out at room temperature. The precipitate generated through the reactions was gathered by filtration, and the solid components obtained here were dried under reduced pressure, to form 9.86 g of 3-(tritylthio)propionic acid 14, which is a white solid.

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