반응 #531788
ord-4352c6a372534f1d85c587f7a1676115
반응 방정식
1,3-bis(2,7,9-triphenyl-1,4,5,6-tetrahydropyrido[3,2-h]quinazolin-4-yl)benzene
→
1,3-bis(2,7,9-triphenylpyrido[3,2-h]quinazolin-4-yl)benzene
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1온도was heated until total dissolution
- 2온도the reaction was refluxed for 6 hours with argon bubbling directly in the solution
실험 절차
A suspension of 1,3-bis(2,7,9-triphenyl-1,4,5,6-tetrahydropyrido[3,2-h]quinazolin-4-yl)benzene (5) (4.4 mmol) in 220 diethyleneglycol was heated until total dissolution. 1.2 g Pd/C was then slowly added, and the reaction was refluxed for 6 hours with argon bubbling directly in the solution. The reaction was then stopped, and the suspension cooled to room temperature.