반응 #52595

반응 방정식

5-amino-2-oxindole

4-methoxycarbonylbenzoyl chloride

→

5-(4-methoxycarbonylbenzamido)-2oxindole

수율 81.0%

용매

pyridine

반응 조건

후처리

1. 1
   여과The precipitate was filtered
2. 2
   세척washed with water
3. 3
   기타dried in a vacuum oven

실험 절차

A mixture of 82.0 mg 5-amino-2-oxindole and 131.0 mg 4-methoxycarbonylbenzoyl chloride in pyridine was stirred at room temperature for 3 hr and poured into ice water. The precipitate was filtered, washed with water and dried in a vacuum oven to give 138.0 mg of 5-(4-methoxycarbonylbenzamido)-2oxindole (81% yield).

출처